Menù principale
B006885 - ORGANIC CHEMISTRY LABORATORY II
Main information
Teaching Language
Course Content
Suggested readings
Learning Objectives
Prerequisites
Teaching Methods
Further information
Type of Assessment
Course program
Academic Year 2022-23
Coorte 2021 - 3-years First Cycle Degree (DM 270/04) in CHIMICA
Course year
Second year - Second Semester
Belonging Department
Chemistry "Ugo Schiff"
Modulo di sola Frequenza of
Scientific Area
CHIM/06 - ORGANIC CHEMISTRY
Credits
6
Teaching Hours
64
Teaching Term
20/02/2023 ⇒ 12/06/2023
Attendance required
Yes
Type of Evaluation
Giudizio Finale
Course Content
show
Course program
show
Lectureship
- Last names A-K MARRADI MARCO
- Last names A-K MATASSINI CAMILLA
- Last names L-Z VIGLIANISI CATERINA
Teaching Language - Last names A-K
italian
Teaching Language - Last names L-Z
italian
Course Content - Last names A-K
Laboratory techniques. Carrying out reactions described in the theoretical course "Organic Chemistry II".
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data (1H NMR, 13C NMR, IR, Massa). Design of a multi-step synthesis.
Disconnection approach: theory and exercises.
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data (1H NMR, 13C NMR, IR, Massa). Design of a multi-step synthesis.
Disconnection approach: theory and exercises.
Course Content - Last names L-Z
Laboratory techniques. Carrying out reactions described in the theoretical course "Organic Chemistry II".
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data (1H NMR, 13C NMR, IR, Massa). Design of a multi-step synthesis.
Disconnection approach: theory and exercises.
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data (1H NMR, 13C NMR, IR, Massa). Design of a multi-step synthesis.
Disconnection approach: theory and exercises.
Suggested readings - Last names A-K (Search our library's catalogue)
Professors' lecture notes.
Identificazione spettrometrica di composti organici - Silverstein R. M. (Casa Editrice Ambrosiana)
Guida Pratica alla Interpretazione di Spettri NMR (Loghìa)
Chimica Organica - W.H. Brown (EdiSES)
Organic Chemistry - Smith J. G. (Mc Graw Hill)
Identificazione spettrometrica di composti organici - Silverstein R. M. (Casa Editrice Ambrosiana)
Guida Pratica alla Interpretazione di Spettri NMR (Loghìa)
Chimica Organica - W.H. Brown (EdiSES)
Organic Chemistry - Smith J. G. (Mc Graw Hill)
Suggested readings - Last names L-Z (Search our library's catalogue)
Professors' lecture notes.
Identificazione spettrometrica di composti organici - Silverstein R. M. (Casa Editrice Ambrosiana)
Guida Pratica alla Interpretazione di Spettri NMR (Loghìa)
Chimica Organica - W.H. Brown (EdiSES)
Organic Chemistry - Smith J. G. (Mc Graw Hill)
Identificazione spettrometrica di composti organici - Silverstein R. M. (Casa Editrice Ambrosiana)
Guida Pratica alla Interpretazione di Spettri NMR (Loghìa)
Chimica Organica - W.H. Brown (EdiSES)
Organic Chemistry - Smith J. G. (Mc Graw Hill)
Learning Objectives - Last names A-K
Gain practical experience in basic techniques of synthesis and purification of organic compounds.
Basic theory of mass spectrometry and 1H NMR and 13C NMR spectroscopy.
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data. Design of a multi-step synthesis.
Basic theory of mass spectrometry and 1H NMR and 13C NMR spectroscopy.
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data. Design of a multi-step synthesis.
Learning Objectives - Last names L-Z
Gain practical experience in basic techniques of synthesis and purification of organic compounds.
Basic theory of mass spectrometry and 1H NMR and 13C NMR spectroscopy.
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data. Design of a multi-step synthesis.
Basic theory of mass spectrometry and 1H NMR and 13C NMR spectroscopy.
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data. Design of a multi-step synthesis.
Prerequisites - Last names A-K
Courses required: none
Courses recommended: Organic Chemistry I and Organic Chemistry Lab. I.
Courses recommended: Organic Chemistry I and Organic Chemistry Lab. I.
Prerequisites - Last names L-Z
Courses required: none
Courses recommended: Organic Chemistry I and Organic Chemistry Lab. I.
Courses recommended: Organic Chemistry I and Organic Chemistry Lab. I.
Teaching Methods - Last names A-K
Contact hours for: Lectures (hours): 16
Contact hours for: Laboratory (hours): 48
Contact hours for: Laboratory (hours): 48
Further information - Last names A-K
Laboratory attendance: mandatory
Lesson attendance: mandatory
Lesson attendance: mandatory
Further information - Last names L-Z
Laboratory attendance: mandatory
Lesson attendance: mandatory for 8 lessons
Lesson attendance: mandatory for 8 lessons
Type of Assessment - Last names A-K
Report on the syntheses carried out in laboratory including characterization of the synthesized products and intermediates.
Written test concerning:
a) theory of mass spectrometry and 1H and 13C NMR spectroscopy
b) structural determination of an unknown organic compound using its spectroscopic data and interpretation of the corresponding spectra
c) retrosynthetic analysis of organic compounds
Successful completion of this test is a prerequisite for the oral exam of "Organic Chemistry II"
Written test concerning:
a) theory of mass spectrometry and 1H and 13C NMR spectroscopy
b) structural determination of an unknown organic compound using its spectroscopic data and interpretation of the corresponding spectra
c) retrosynthetic analysis of organic compounds
Successful completion of this test is a prerequisite for the oral exam of "Organic Chemistry II"
Type of Assessment - Last names L-Z
Report on the syntheses carried out in laboratory including characterization of the synthesized products and intermediates.
Written test concerning:
a) theory of mass spectrometry and 1H and 13C NMR spectroscopy
b) structural determination of an unknown organic compound using its spectroscopic data and interpretation of the corresponding spectra
c) retrosynthetic analysis of organic compounds
Successful completion of this test is a prerequisite for the oral exam of "Organic Chemistry II"
Written test concerning:
a) theory of mass spectrometry and 1H and 13C NMR spectroscopy
b) structural determination of an unknown organic compound using its spectroscopic data and interpretation of the corresponding spectra
c) retrosynthetic analysis of organic compounds
Successful completion of this test is a prerequisite for the oral exam of "Organic Chemistry II"
Course program - Last names A-K
Laboratory techniques. Carrying out reactions described in the theoretical course "Organic Chemistry II".
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data (1H NMR, 13C NMR, IR, Massa). Design of a multi-step synthesis.
Disconnection approach: theory and exercises.
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data (1H NMR, 13C NMR, IR, Massa). Design of a multi-step synthesis.
Disconnection approach: theory and exercises.
Course program - Last names L-Z
Laboratory techniques. Carrying out reactions described in the theoretical course "Organic Chemistry II".
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data (1H NMR, 13C NMR, IR, Massa). Design of a multi-step synthesis.
Disconnection approach: theory and exercises.
Interpretation of 1H NMR, 13C NMR and mass spectra. Structural determination of unknown organic compounds through their spectroscopic data (1H NMR, 13C NMR, IR, Massa). Design of a multi-step synthesis.
Disconnection approach: theory and exercises.